SOLUTION NMR
| NMR Experiment | ||||||||
|---|---|---|---|---|---|---|---|---|
| Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
| 1 | 3D_13C-separated_NOESY | 1MM ADR6 ARID DOMAIN U-15N, U-13C, 50MM PHOSPHATE BUFFER PH4.9, 90% H2O, 10%D2O | 90% H2O/10% D2O | 50mM PHOSPHATE BUFFER | 4.9 | ambient | 300 | |
| 2 | 3D_15N-separated_NOESY | |||||||
| 3 | 2D NOESY | |||||||
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | Bruker | DMX | 500 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| torsion angle dynamics | CNS | |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | |
| Conformers Calculated Total Number | |
| Conformers Submitted Total Number | 1 |
| Representative Model | 1 (minimized average structure) |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | CNS | v 1.0 | A.T. BRUNGER |
