C-TERMINAL HALF OF VACCINIA VIRUS COMPLEMENT CONTROL PROTEIN, NMR, MINIMIZED AVERAGE STRUCTURE
SOLUTION NMR
| NMR Experiment | ||||||||
|---|---|---|---|---|---|---|---|---|
| Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
| 1 | 15N | 4.0 | 310 | |||||
| 2 | 1H-NOESY HSQC | 4.0 | 310 | |||||
| 3 | 15N | 4.0 | 310 | |||||
| 4 | 1H-TOCSY HSQC | 4.0 | 310 | |||||
| 5 | DQF-COSY | 4.0 | 310 | |||||
| 6 | NOESY | 4.0 | 310 | |||||
| 7 | HOHAHA | 4.0 | 310 | |||||
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | HOME BUILT/GE | home-built | 750 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| SIMULATE ANNEALING | REFINEMENT DETAILS CAN BE FOUND IN THE JRNL CITATION. | X-PLOR |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | < 2 NOE VIOLATIONS > 0.5 A; NO DIHEDRAL ANGLE VIOLATIONS > 5 DEGREES |
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 1 |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | X-PLOR | 3.84 | BRUNGER |
| 2 | structure solution | X-PLOR | ||
