SOLUTION STRUCTURE OF REDUCED MICROSOMAL RAT CYTOCHROME B5, NMR, MINIMIZED AVERAGE STRUCTURE
SOLUTION NMR
| NMR Experiment | ||||||||
|---|---|---|---|---|---|---|---|---|
| Experiment | Type | Sample Contents | Solvent | Ionic Strength | pH | Pressure | Temperature (K) | Spectrometer |
| 1 | NOESY WATERGATE | 7 | 313 | |||||
| 2 | TOCSY | 7 | 313 | |||||
| 3 | COSY | 7 | 313 | |||||
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | Bruker | AVANCE 800 MHZ | 800 |
| 2 | Bruker | AMX 600 MHZ | 600 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| TORSION ANGLE MOLECULAR DYNAMICS SIMULATED ANNEALING, RESTRAINED ENERGY MINIMIZATION | DIANA | |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | MINIMIZED AVERAGE |
| Conformers Calculated Total Number | 40 |
| Conformers Submitted Total Number | 1 |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | DIANA | WUTHRICH | |
| 2 | structure solution | DYANA | ||
| 3 | structure solution | Amber | ||
