Solution structure of the a-subunit of human chorionic gonadotropin [modeled without carbohydrate residues]
SOLUTION NMR
| NMR Spectrometer Information | |||
|---|---|---|---|
| Spectrometer | Manufacturer | Model | Field Strength |
| 1 | Bruker | AMX | 500 |
| 2 | Bruker | DRX | 600 |
| 3 | Varian | UNITYPLUS | 750 |
| NMR Refinement | ||
|---|---|---|
| Method | Details | Software |
| DG/SA | SPECIAL REFINEMENT PROCEDURE TO OPTIMIZE CONVERGENCE RATE OF THE CYSTINE KNOT FORMATION | X-PLOR |
| NMR Ensemble Information | |
|---|---|
| Conformer Selection Criteria | |
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 27 |
| Additional NMR Experimental Information | |
|---|---|
| Details | STRUCTURAL STATISTICS FOR THE FAMILY OF 27 AHCG CONFORMERS EXCLUDE THE FLEXIBLE LOOP AND ENDS, SEGMENTS 1-10, 29-58 AND 85-92 (SEE REFERENCE) |
| Computation: NMR Software | ||||
|---|---|---|---|---|
| # | Classification | Version | Software Name | Author |
| 1 | refinement | X-PLOR | 3.851 | BRUNGER |
| 2 | structure solution | X-PLOR | ||
